Thermal Analysis

TGA

Thermogravimetric Analysis

TGA weighs a sample continuously as it is heated. The mass-loss steps show moisture and volatiles, decomposition temperatures and the final residue, such as filler or ash content.

3 test optionsMicrogram mass resolutionRoom temperature to 1500 °CTypical turnaround 3–5 working days
TGA measurement principleIllustrative
MicrobalanceFurnaceSample panPurge gasThermocoupleMassTemperature
A sample, weighed as it is heatedIllustrative
01 / Overview

What is TGA?

Thermogravimetric Analysis places a few milligrams of sample on a sensitive microbalance inside a furnace. As the temperature rises at a set rate, the balance records every change in mass, so evaporation, dehydration, decomposition and oxidation each appear as a step in the curve.

TGA is the quickest way to find how much of a material is moisture, organic matter or inorganic residue, and at what temperature it becomes unstable. Switching the gas from nitrogen to air helps separate polymer, carbon and filler. It cannot see events without a mass change, such as melting.

02 / How it works

How it works

  1. 01

    Sample is loaded

    A few milligrams are placed in a small crucible and the balance is tared.

  2. 02

    Weighed while heated

    The crucible hangs from a microbalance inside the furnace, under a gas purge.

  3. 03

    Mass is tracked

    As the furnace heats at a steady rate, the balance records every change in mass.

  4. 04

    Steps are measured

    Each step gives a mass loss in %, and the plateau at the end gives the residue.

03 / What it measures

What it measures

Moisture & volatile content

Mass lost at low temperature as water and solvents leave.

Useful forPowders, polymers, pharmaceuticals

Thermal stability

The onset temperature at which the material starts to decompose.

Useful forPolymers, drugs, organics

Filler, ash & residue content

Inorganic residue left once organic matter has burnt off.

Useful forFilled plastics, composites, rubber

Multi-component composition

Polymer, carbon black and filler fractions from successive steps.

Useful forRubber compounds, blends

Organic loading on particles

Amount of coating, ligand or drug carried on nanoparticles.

Useful forFunctionalised nanomaterials, carriers

Oxidation & mass gain

Mass increase as metals or alloys oxidise in air.

Useful forMetals, alloys, oxidation resistance
04 / Test options

Choose the TGA options you need

3 options · none added yet

TGA test options
05 / Sample requirements

Sample requirements

Accepted forms
Powders, granules, films, fibres, small solid pieces and liquids
Quantity
At least 50 mg per sample (5–20 mg is used per run)
Piece size
Small enough to lie flat in a ~5 mm crucible
Liquids
Sent in sealed vials; mention if volatile
  • Dry samples, unless moisture content is part of the study
  • State the atmosphere (nitrogen or air) and end temperature you need
  • Send in sealed, labelled vials
  • No explosive, energetic or self-reactive materials
  • No samples releasing corrosive or toxic gases without prior discussion

Hazardous or air-sensitive samples: mention it in your request, and attach the MSDS if you have one.

06 / Results & turnaround

Results & turnaround

What you receive

  • TGA curve (mass % vs temperature)
  • DTG (derivative) curve
  • Mass loss per step and final residue (%)
  • Onset and decomposition temperatures
  • Raw data files
  • Report PDF

Turnaround & pricing

Typically 3–5 working days after samples reach the lab.

Price confirmed in your quotation, depending on user type, options and number of samples.

Sample report · IllustrativeExample residue at 700 °C18.6 %Illustrative — not measured sample data
07 / Limitations

When TGA isn't the right fit

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