Elemental & Composition

EDX / EDS

Energy Dispersive Spectroscopy

EDX identifies the elements in a sample from the characteristic X-rays it emits under an electron beam. It gives fast, semi-quantitative composition of a spot, area or map, usually alongside SEM imaging.

1 test optionDetects elements from ~B to UDetection limit ~0.1–1 wt%Typical turnaround 4–6 working days
EDX / EDS measurement principleIllustrative
Electron beamShell transitionX-raysEDX detectorSampleSpectrum
Every element, its own X-ray signatureIllustrative
01 / Overview

What is EDX / EDS?

When the electron beam of an SEM or TEM strikes a sample, it knocks inner-shell electrons out of atoms. As outer electrons drop into the gaps, each element emits X-rays at its own characteristic energies, and an energy-dispersive detector sorts them into a spectrum of peaks.

EDX analyses a feature you can see in the image, and can map how elements are spread across it, which bulk methods such as XRF or ICP cannot. Results are semi-quantitative, detection limits are typically 0.1–1 wt%, and H, He and Li cannot be detected.

02 / How it works

How it works

  1. 01

    Sample goes into the SEM

    The sample is mounted on a stub under the beam; insulators get a thin carbon coat.

  2. 02

    Beam excites atoms

    The focused electron beam knocks inner-shell electrons out of atoms in a small volume.

  3. 03

    X-rays are sorted

    Each element emits X-rays at its own energies; the detector counts them by energy.

  4. 04

    Spectrum and maps

    Peaks are identified and quantified, or the beam is scanned to map each element.

03 / What it measures

What it measures

Elements present

Identify which elements are in a spot, area or particle.

Useful forUnknown residues, contaminants, minerals

Semi-quantitative composition

Estimate the wt% and at% of the detected elements.

Useful forAlloys, ceramics, catalysts, coatings

Point & area analysis

Target a single particle, inclusion or region you can see in the image.

Useful forInclusions, defects, individual particles

Line scans

Follow how composition changes across an interface or coating.

Useful forCoatings, diffusion zones, joints

Elemental maps

Show where each element sits across the imaged area.

Useful forSegregation, dopants, coating coverage
04 / Test options

Choose the EDX / EDS options you need

1 option · none added yet

EDX / EDS test options
05 / Sample requirements

Sample requirements

Accepted forms
Powders, films, fibres, solid pieces, polished sections
Size
Up to ~20 × 20 mm, height under 10 mm
Quantity
About 10 mg of powder; one piece per sample
Surface
Flat, polished surfaces give the most reliable numbers
Condition
Dry, vacuum-stable, free of solvents and oils
  • Fully dry samples, free of solvents and moisture
  • Powders in sealed, labelled vials
  • Mark the spot or region you want analysed
  • List the elements you expect or need checked
  • No liquids, gels or wet samples
  • No samples that outgas or decompose in vacuum

Hazardous or air-sensitive samples: mention it in your request, and attach the MSDS if you have one.

06 / Results & turnaround

Results & turnaround

What you receive

  • EDX spectra with identified element peaks
  • Semi-quantitative wt% and at% tables
  • Image showing where each analysis was taken
  • Raw spectrum files
  • Report PDF

Turnaround & pricing

Typically 4–6 working days after samples reach the lab.

Price confirmed in your quotation, depending on user type, options and number of samples.

Sample report · IllustrativeExample Cr content18.2 wt%Illustrative — not measured sample data
07 / Limitations

When EDX / EDS isn't the right fit

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